by Joseph
Braze Fixturing via Tack-welding — the Good and the Bad!
Highly complex assemblies, for a variety of end-use applications in such diverse fields as automotive, aerospace, medical, electronics, and tooling (just to name a few), can be effectively made via brazing.
For this to happen, however, each of the individual components in these complex assemblies must be able to be held together in proper alignment, have the appropriate brazing filler metal (BFM) applied to it, and this assembly then moved into a brazing-furnace, where it can be heated until the BFM melts and flows into the joints by capillary action, thereby permanently joining the components together to make a complex assembly. by Dan Kay
by George Vander Voort
Use of the Scanning Electron Microscope in Failure Analysis
Commercial introduction of the Scanning Electron Microscope (SEM) in 1965, and its subsequent rapid development and implementation in metallographic laboratories, has had a profound influence on failure studies. The chief advantage of the SEM is its great depth of field in comparison of the light microscope. Observations can be made over a much wider range of magnifications including those above the range for light microscopes (and those below the range of TEM replicas). Examination of fracture features by SEM is much simpler than through the study of replicas with the Transmission Electron Microscope, TEM. A further advantage of the SEM is the chemical analytical capability of spectrometers that can be attached to the microscope, Energy-dispersive Spectrometers (EDS) being the most common.
The study of fractures with the unaided eye has been practiced since antiquity chiefly for controlling the quality of metals production. R. A. F. de Réammur may have been the first to examine and publish drawings of fractures examined at high magnifications, at least 100X, in 1722. R. Mallet appears to have been the first to link fracture appearance to service performances in a study of failed cannon barrels published in 1856. Adolf Martens may have been the first to study both fracture surfaces and the underlying microstructures in 1878 followed by the first description of fracture surface features in 1887 when he showed that these lineal features could be traced backward to identify the fracture origin. By George Vander Voort
by Joseph
Oil for Vacuum Pumps
In the world of mechanical oil sealed rotary vacuum pumps there is a need for a variety of oils and fluids to suit the specific type of pump, its duty and the process it is used on. This discussion covers high vacuum pumps only, such as are used in the heat treating and vacuum furnace industry. These same vacuum pumps are used in many other industrial and scientific applications and have to work under many different types of conditions including one that many people expose their pumps too – neglect!.
Rotary vane vacuum pumps are available as direct drive (usually 1800 rpm) and vee belt drive (between 400 and 500 rpm) versions. Rotary piston vacuum pumps are generally vee belt driven and run at about 500 rpm. The work duty of a vacuum pump can vary between intermittent use and running continuously. They can also be used for cyclic duty, to evacuate a loadlock for example, where the pump evacuates a chamber from atmosphere to vacuum every few minutes. The vacuum process can also vary, from clean air pumping to hazardous gas, wet vapor pumping and dirty/dusty atmospheres.. By Howard Tring
by George Vander Voort
Safety in the Metallography Laboratory
The metallographic laboratory is a relatively safe working environment; however, there are dangers inherent to the job. Included in these dangers is exposure to heat, acids, bases, oxidizers and solvents. Specimen preparation devices, such as drill presses, shears and cutoff saws, also present hazards. In general, these dangers can be minimized if the metallographer consults documents such as ASTM E 2014 (Standard Guide on Metallographic Laboratory Safety) and relevant Material Safety Data Sheets (MSDS) before working with unfamiliar chemicals. Common sense, caution, training in basic laboratory skills, a laboratory safety program, access to safety reference books – these are some of the ingredients of a recipe for laboratory safety.
Safe working habits begin with good housekeeping. A neat, orderly laboratory promotes safe working habits, while a sloppy, messy work area invites disaster. Good working habits include such obvious, commonsense items as washing the hands after handling chemicals or before eating. Simple carelessness can cause accidents. For example, failure to clean glassware after use can cause an accident for the next user. Another common problem is burns due to failure to properly clean acid spills or splatter. By George Vander Voort
by Joseph
Vacuum Heat Treatment of Fasteners
Fastener applications are demanding. Whether fasteners are being used in the petrochemical industry, in medical or mining applications, for assembly of marine or nuclear components or in the aerospace, automotive or construction world, vacuum processing allows us to repeatedly achieve the highest quality and metallurgy.
Most fastener materials, including stainless steels and superalloy grades, benefit from or actually require vacuum processing for heat treatment instead of being run under protective atmospheres. In general, there are three main sets of applications that where vacuum heat treatment is used: processes that can be done in no other way than in vacuum; processes that can be done better in vacuum from a metallurgical standpoint or processes that can be done better in vacuum from an economic standpoint. By Dan Herring
by Joseph
Brazing Filler Metal (BFM) “Certification of Conformance” – Have you ever had a problem with one?
by Dan Kay
This is a question that arises once in a while, and needs to be taken seriously. Fortunately, for most of us, problems with Certificates of Conformance (or Certificate of Compliance) are very rare. Most manufacturers of brazing filler metals (BFMs) are reputable companies who pride themselves in being able to produce high-quality BFMs in such a way that the BFM product is homogeneous, and its chemistry is carefully controlled in a manner that can guarantee that it fully meets the requirements of the specification(s) to which it is being produced.
The Certificate of Conformance will show the BFM specification(s) to which it conforms, and the customer to whom the “cert” was sent should be able to fully rely on the accuracy and truthfulness of that document. Every once in a while, a customer, using a BFM product (paste, wire, preform, etc.) which they have purchased from their supplier, discovers that the BFM product does not perform the way it is supposed to, and many questions begin to surface about that product they have received.
by Joseph
VAC AERO Sells Vacuum Furnace to Southeast Asian Aerospace Manufacturer.
Burlington, Ontario, December 15, 2014 – VAC AERO has sold a VAH4848 HV-6 high-pressure quench vacuum furnace to a manufacturer and integrator of high performance aerospace systems and components. The furnace is designed to have rapid heating rates while maintaining tight uniformity at high vacuum levels and is equipped with a gas quench system capable of quench pressures up to six bar. The furnace features a 36” wide x 30” high x 48” long carbon hot zone with a heavy duty hearth designed to support a uniformly distributed load of 2500 lbs. VAC AERO’s decades of experience operating aerospace heat treating facilities allows them to offer customers training, technology transfer as well as hands-on instruction and collaboration.
by Joseph
Maintenance of Vacuum Furnaces – Part Three
We continue our discussion on the maintenance of vacuum furnaces. In Parts One and Two we talked about establishing a sound maintenance strategy, implementing that strategy and working on critical components of the vacuum system to return the unit to full operational status. Let’s continue this discussion.
General Maintenance – The following additional topics comprise the critical areas and systems that routinely require maintenance to ensure they operate correctly. Hot Zone Maintenance – After ensuring proper ventilation and following all safety guidelines with respect to asphyxiation and confined space entry, the interior of the hot zone should be inspected after every load. The bottom of the hot zone should be cleaned of all debris and foreign matter and the heating elements and heating element connections inspected for damage and tightness. Graphite heating elements can in some instances be patched and the damaged section replaced with a new element section. Molybdenum heating elements can be repaired although no more than three (3) repairs are recommended per element band. By Dan Herring.
by Joseph
Why is a nitrogen atmosphere disallowed when nickel-brazing per AMS 2675?
by Dan Kay
In AMS 2675G (“Brazing, using Nickel-Alloy Filler Metal”), paragraph 3.3 states that acceptable atmospheres for nickel-brazing are hydrogen, argon, or vacuum. No mention of nitrogen. People have asked me why nitrogen is apparently not allowed for furnace brazing with nickel-based brazing filler metals (BFMs), or for building up partial-pressures in a vacuum furnace for subsequent brazing.
ANSWER: Nitrogen, like hydrogen, can be reactive towards some of the metallic components in the base-metals and in the liquid BFM during brazing processes. As a safe-guard against any such problems, AMS 2675 excludes nitrogen from its list of acceptable furnace atmospheres for nickel-brazing. Will nitrogen ALWAYS be a problem in nickel-brazing in a furnace atmosphere? NO! Please be aware that the exclusion of nitrogen is a “general safety” recommendation (suggestion), and is not to be taken as a prohibition against nitrogen for any and all nickel-brazing. Let’s take a closer look…….
by George Vander Voort
Selective Etching and Quantitative Measurements Used to Assess the Thermal Exposure to the Lower Head of the Three-Mile Island Unit 2 Nuclear Reactor
The accident at Unit No. 2 of the Three Mile Island nuclear reactor (TMI-2) on March 28, 1979 was the worst nuclear accident in US history and crippled the nuclear industry. It was not possible to remove specimens from the lower head until January – March 1990. Fourteen of the fifteen specimens removed by electrical discharge machining were from under the debris pile that accumulated on the lower head due to melting of ~19,000 kg (~45%) of the core. Specimens were previously cut from the lower head of a cancelled reactor of very similar size and design destined for Midland, Michigan. These specimens were subjected to controlled heating cycles with peak temperatures from 800 to 1100°C for periods of 1 to 100 minutes. The writer examined both sets of specimens and employed selective etching followed by quantitative metallography (by image analysis) to obtain a far more detailed description of the thermal exposure experienced than had been obtained previously. By George Vander Voort